Solvothermal Synthesis, Crystal Structure and Luminescence Property of a 1D Silver(I) Coordination Polymer

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摘要 An unprecedented one-dimensional coordination polymer [Ag2(PhPO3H)2(DPPP)]n (1) based on phenylphosphonic acid (PhPO3H2) and 1,3-bis(diphenyphosphino)propane (DPPP) has been synthesized and characterized by IR, elemental analyses, thermogravimetric analyses and X-ray diffraction technique. Single-crystal X-ray diffraction analyses revealed that the complex crystallizes in triclinic system, space group P(-). The coordination geometry of each Ag(I) ion is planar trigonal. Two kinds of rings were found in 1, such as the four-membered ring with Ag2O2 and the eight-membered ring with Ag2O4P2 constructed by PhPO3H– ligands, which were then connected by DPPP ligands forming a zigzag type chain. Moreover, the light absorption and luminescent property of 1 were also investigated.

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	张楠
	郭玉华
	郁有祝
	王振
	牛永生
	武现丽

关键词 ： silver, crystal structure, coordination polymer, photoluminescent property

Abstract：An unprecedented one-dimensional coordination polymer [Ag2(PhPO3H)2(DPPP)]n (1) based on phenylphosphonic acid (PhPO3H2) and 1,3-bis(diphenyphosphino)propane (DPPP) has been synthesized and characterized by IR, elemental analyses, thermogravimetric analyses and X-ray diffraction technique. Single-crystal X-ray diffraction analyses revealed that the complex crystallizes in triclinic system, space group P(-). The coordination geometry of each Ag(I) ion is planar trigonal. Two kinds of rings were found in 1, such as the four-membered ring with Ag2O2 and the eight-membered ring with Ag2O4P2 constructed by PhPO3H– ligands, which were then connected by DPPP ligands forming a zigzag type chain. Moreover, the light absorption and luminescent property of 1 were also investigated.

Key words： silver crystal structure coordination polymer photoluminescent property

收稿日期: 2020-02-01 出版日期: 2020-11-09

基金资助:This work was financially supported by the National Natural Science Foundation of China (No. 21702005), the Foundation of the Henan Joint International Research Laboratory of Nanocomposite Sensing Materials and the Foundation of Anyang Institute of Technology (YPY2019003)

通讯作者: 119yyz@163.com E-mail: 119yyz@163.com

引用本文:

张楠;郭玉华;郁有祝;王振;牛永生;武现丽. Solvothermal Synthesis, Crystal Structure and Luminescence Property of a 1D Silver(I) Coordination Polymer[J]. 结构化学, 2020, 39(11): 2009-2015.
ZHANG Nan;GUO Yu-Hua;YU You-Zhu;WANG Zhen;NIU Yong-Sheng;WU Xian-Li. Solvothermal Synthesis, Crystal Structure and Luminescence Property of a 1D Silver(I) Coordination Polymer. CHINESE JOURNAL OF STRUCTURAL CHEMISTRY, 2020, 39(11): 2009-2015.

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http://manu30.magtech.com.cn/jghx/CN/ 或 http://manu30.magtech.com.cn/jghx/CN/Y2020/V39/I11/2009

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